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Utilizing an ultramicrotome to produce cross-sections of the printed multilayer structure for subsequent <t>SEM</t> imaging: ( a ) cross-sections prepared by Ar-ion beam milling and ultramicrotome trimming viewed in an SEM, scale bar: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$1\,\upmu \hbox {m}$$\end{document} 1 μ m ; ( b ) a non-magnetic flat sample holder for UM (left), the tip of the clamping jaws is trimmed (right) to create a flat opening, and the central borehole of the <t>SEM</t> <t>specimen</t> holder is enlarged to 9.85 mm (center) to mount the UM flat sample holder, diameter of SEM specimen holder, 46 mm; ( c ) the sample is fixed in the UM holder for three times repetitive trimming and SEM imaging, scale bar in top view: 1 mm, in images of sample trimming: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$250\,\upmu \hbox {m}$$\end{document} 250 μ m .
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Utilizing an ultramicrotome to produce cross-sections of the printed multilayer structure for subsequent <t>SEM</t> imaging: ( a ) cross-sections prepared by Ar-ion beam milling and ultramicrotome trimming viewed in an SEM, scale bar: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$1\,\upmu \hbox {m}$$\end{document} 1 μ m ; ( b ) a non-magnetic flat sample holder for UM (left), the tip of the clamping jaws is trimmed (right) to create a flat opening, and the central borehole of the <t>SEM</t> <t>specimen</t> holder is enlarged to 9.85 mm (center) to mount the UM flat sample holder, diameter of SEM specimen holder, 46 mm; ( c ) the sample is fixed in the UM holder for three times repetitive trimming and SEM imaging, scale bar in top view: 1 mm, in images of sample trimming: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$250\,\upmu \hbox {m}$$\end{document} 250 μ m .
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Utilizing an ultramicrotome to produce cross-sections of the printed multilayer structure for subsequent SEM imaging: ( a ) cross-sections prepared by Ar-ion beam milling and ultramicrotome trimming viewed in an SEM, scale bar: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$1\,\upmu \hbox {m}$$\end{document} 1 μ m ; ( b ) a non-magnetic flat sample holder for UM (left), the tip of the clamping jaws is trimmed (right) to create a flat opening, and the central borehole of the SEM specimen holder is enlarged to 9.85 mm (center) to mount the UM flat sample holder, diameter of SEM specimen holder, 46 mm; ( c ) the sample is fixed in the UM holder for three times repetitive trimming and SEM imaging, scale bar in top view: 1 mm, in images of sample trimming: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$250\,\upmu \hbox {m}$$\end{document} 250 μ m .

Journal: Scientific Reports

Article Title: Repetitive ultramicrotome trimming and SEM imaging for characterizing printed multilayer structures

doi: 10.1038/s41598-024-79717-0

Figure Lengend Snippet: Utilizing an ultramicrotome to produce cross-sections of the printed multilayer structure for subsequent SEM imaging: ( a ) cross-sections prepared by Ar-ion beam milling and ultramicrotome trimming viewed in an SEM, scale bar: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$1\,\upmu \hbox {m}$$\end{document} 1 μ m ; ( b ) a non-magnetic flat sample holder for UM (left), the tip of the clamping jaws is trimmed (right) to create a flat opening, and the central borehole of the SEM specimen holder is enlarged to 9.85 mm (center) to mount the UM flat sample holder, diameter of SEM specimen holder, 46 mm; ( c ) the sample is fixed in the UM holder for three times repetitive trimming and SEM imaging, scale bar in top view: 1 mm, in images of sample trimming: \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$250\,\upmu \hbox {m}$$\end{document} 250 μ m .

Article Snippet: To make the sample holder directly applicable for SEM imaging, the central borehole of an SEM specimen holder (Carl Zeiss Microscopy Deutschland GmbH, Germany) is enlarged to 9.85 mm, which is the diameter of the cylindrical shaft of the UM flat sample holder.

Techniques: Imaging