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rotation electron diffraction cred data  (Gatan Inc)
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Rotation Electron Diffraction Cred Data, supplied by Gatan Inc, used in various techniques. Bioz Stars score: 99/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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rotation electron diffraction cred data  (JEOL)
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JEOL rotation electron diffraction cred data
The cut distance of HCA is represented in dendrogram by the blue line at 0.5 for E-FCOF-5 ( a ) and 0.56 C-FCOF-5 ( c ), which results in 16 <t>cRED</t> datasets belonging to the largest cluster for E-FCOF-5 ( a , in red) and E-FCOF-5 ( c , in red). The overview of 3D reciprocal lattices of E-FCOF-5 ( b ) and C-FCOF-5 ( d ) merged from 16 cRED datasets. The observed potential density maps of E-FCOF-5 ( e ) and C-FCOF-5 ( g ). The structures were refined isotropically using soft restraints for the geometry of the phenyl rings as well as the C–C and C=N bond lengths. The observed peaks appeared to be spherical with similar peak heights for the same atom types. The porous structure of E-FCOF-5 ( f -up) and C-FCOF-5 ( h -up). The single pts net of E-FCOF-5 ( f -down) and C-FCOF-5 ( h -down).
Rotation Electron Diffraction Cred Data, supplied by JEOL, used in various techniques. Bioz Stars score: 99/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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continuous rotation electron diffraction cred data  (JEOL)
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JEOL continuous rotation electron diffraction cred data
The cut distance of HCA is represented in dendrogram by the blue line at 0.5 for E-FCOF-5 ( a ) and 0.56 C-FCOF-5 ( c ), which results in 16 <t>cRED</t> datasets belonging to the largest cluster for E-FCOF-5 ( a , in red) and E-FCOF-5 ( c , in red). The overview of 3D reciprocal lattices of E-FCOF-5 ( b ) and C-FCOF-5 ( d ) merged from 16 cRED datasets. The observed potential density maps of E-FCOF-5 ( e ) and C-FCOF-5 ( g ). The structures were refined isotropically using soft restraints for the geometry of the phenyl rings as well as the C–C and C=N bond lengths. The observed peaks appeared to be spherical with similar peak heights for the same atom types. The porous structure of E-FCOF-5 ( f -up) and C-FCOF-5 ( h -up). The single pts net of E-FCOF-5 ( f -down) and C-FCOF-5 ( h -down).
Continuous Rotation Electron Diffraction Cred Data, supplied by JEOL, used in various techniques. Bioz Stars score: 99/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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The cut distance of HCA is represented in dendrogram by the blue line at 0.5 for E-FCOF-5 ( a ) and 0.56 C-FCOF-5 ( c ), which results in 16 cRED datasets belonging to the largest cluster for E-FCOF-5 ( a , in red) and E-FCOF-5 ( c , in red). The overview of 3D reciprocal lattices of E-FCOF-5 ( b ) and C-FCOF-5 ( d ) merged from 16 cRED datasets. The observed potential density maps of E-FCOF-5 ( e ) and C-FCOF-5 ( g ). The structures were refined isotropically using soft restraints for the geometry of the phenyl rings as well as the C–C and C=N bond lengths. The observed peaks appeared to be spherical with similar peak heights for the same atom types. The porous structure of E-FCOF-5 ( f -up) and C-FCOF-5 ( h -up). The single pts net of E-FCOF-5 ( f -down) and C-FCOF-5 ( h -down).

Journal: Nature Communications

Article Title: Atomic-resolution structures from polycrystalline covalent organic frameworks with enhanced cryo-cRED

doi: 10.1038/s41467-022-31524-9

Figure Lengend Snippet: The cut distance of HCA is represented in dendrogram by the blue line at 0.5 for E-FCOF-5 ( a ) and 0.56 C-FCOF-5 ( c ), which results in 16 cRED datasets belonging to the largest cluster for E-FCOF-5 ( a , in red) and E-FCOF-5 ( c , in red). The overview of 3D reciprocal lattices of E-FCOF-5 ( b ) and C-FCOF-5 ( d ) merged from 16 cRED datasets. The observed potential density maps of E-FCOF-5 ( e ) and C-FCOF-5 ( g ). The structures were refined isotropically using soft restraints for the geometry of the phenyl rings as well as the C–C and C=N bond lengths. The observed peaks appeared to be spherical with similar peak heights for the same atom types. The porous structure of E-FCOF-5 ( f -up) and C-FCOF-5 ( h -up). The single pts net of E-FCOF-5 ( f -down) and C-FCOF-5 ( h -down).

Article Snippet: The continuous rotation electron diffraction (cRED) data were collected on the JEOL JEM-2100 transmission electron microscope (TEM, Cs : 1.0 mm, point resolution: 0.23 nm) at 200 kV using the instamatic script ( https://github.com/instamatic-dev/instamatic ).

Techniques:

The overview of automatically selected six 3D ED datasets of 3D-TPB-COF-OMe ( a ) and 3D-TPB-COF-Me ( d ) for merging and scaling. The dendrogram shows the results of the hierarchical cluster analysis (HCA) of extracted intensities using the correlation coefficients of the common reflection intensities ( CC I ) between pairs of datasets. The cut distance is represented by the blue line at 0.30 (corresponding to CC I = 0.95) for 3D-TPB-COF-OMe ( b ) and 3D-TPB-COF-Me ( e ). In total, the largest clusters were identified with six cRED datasets for 3D-TPB-COF-OMe ( b , in green) and 3D-TPB-COF-Me ( e , in green), which were selected for the structure determination and refinement. The overview of merged 3D reciprocal lattices of 3D-TPB-COF-OMe ( c ) and 3D-TPB-COF-Me ( f ).

Journal: Nature Communications

Article Title: Atomic-resolution structures from polycrystalline covalent organic frameworks with enhanced cryo-cRED

doi: 10.1038/s41467-022-31524-9

Figure Lengend Snippet: The overview of automatically selected six 3D ED datasets of 3D-TPB-COF-OMe ( a ) and 3D-TPB-COF-Me ( d ) for merging and scaling. The dendrogram shows the results of the hierarchical cluster analysis (HCA) of extracted intensities using the correlation coefficients of the common reflection intensities ( CC I ) between pairs of datasets. The cut distance is represented by the blue line at 0.30 (corresponding to CC I = 0.95) for 3D-TPB-COF-OMe ( b ) and 3D-TPB-COF-Me ( e ). In total, the largest clusters were identified with six cRED datasets for 3D-TPB-COF-OMe ( b , in green) and 3D-TPB-COF-Me ( e , in green), which were selected for the structure determination and refinement. The overview of merged 3D reciprocal lattices of 3D-TPB-COF-OMe ( c ) and 3D-TPB-COF-Me ( f ).

Article Snippet: The continuous rotation electron diffraction (cRED) data were collected on the JEOL JEM-2100 transmission electron microscope (TEM, Cs : 1.0 mm, point resolution: 0.23 nm) at 200 kV using the instamatic script ( https://github.com/instamatic-dev/instamatic ).

Techniques: