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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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Merck KGaA synthetic precipitated calcium carbonate (pcc) spindle-shaped and long particles
ESP (untreated ground eggshell powders) and <t>PCC</t> particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, <t>(F)</t> <t>ATR</t> spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.
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ESP (untreated ground eggshell powders) and PCC particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, (F) ATR spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: ESP (untreated ground eggshell powders) and PCC particles without polyelectrolytes, (A) SEM micro image of ESP, (B) SEM micro image of PCC from 0.5 M concentration, (C) higher magnification of image (A), (D) SEM micro image of PCC from 0.03 M concentration, (E) XRD fingerprints, (F) ATR spectra, and (G) Raman spectra of ESP, (a) PCC from 0.5 M concentration and (b) PCC from 0.03 M concentration.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Concentration Assay

(A) SEM image of PCC from 0.5 M salt concentration and 2 w/v% PEG-600, (B) SEM image of PCC from 0.5 M concentration and 2 w/v% PEG-6000, (C) SEM image of PCC from 0.5 M concentration and 2 w/v% EG, (D) SEM image of PCC from 0.5 M concentration and 1.5 w/v% PSS, (E) XRD fingerprints, (F) ATR spectra and (G) Raman spectra of (a) PCC in presence of 2 w/v% PEG-600, (b) PCC in presence of 2 w/v% PEG-6000, (c) PCC in presence of 2 w/v% EG and (d) PCC in presence of 1.5 w/v% PSS.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: (A) SEM image of PCC from 0.5 M salt concentration and 2 w/v% PEG-600, (B) SEM image of PCC from 0.5 M concentration and 2 w/v% PEG-6000, (C) SEM image of PCC from 0.5 M concentration and 2 w/v% EG, (D) SEM image of PCC from 0.5 M concentration and 1.5 w/v% PSS, (E) XRD fingerprints, (F) ATR spectra and (G) Raman spectra of (a) PCC in presence of 2 w/v% PEG-600, (b) PCC in presence of 2 w/v% PEG-6000, (c) PCC in presence of 2 w/v% EG and (d) PCC in presence of 1.5 w/v% PSS.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Concentration Assay

(A) SEM image of PCC from 0.5 M salt concentration and 4 w/v% EG, (B) SEM image of PCC from 0.5 M salt concentration and 4 w/v% PEG-6000, (C) SEM image of PCC with 0.5 M salt concentration and 7 w/v% PEG-6000. (D) XRD fingerprints, (E) ATR spectra and (F) Raman spectra of (a) PCC in presence of 4 w/v% EG, (b) PCC in presence of 4 w/v% PEG-6000, (c) PCC in presence of 7 w/v% PEG-6000.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: (A) SEM image of PCC from 0.5 M salt concentration and 4 w/v% EG, (B) SEM image of PCC from 0.5 M salt concentration and 4 w/v% PEG-6000, (C) SEM image of PCC with 0.5 M salt concentration and 7 w/v% PEG-6000. (D) XRD fingerprints, (E) ATR spectra and (F) Raman spectra of (a) PCC in presence of 4 w/v% EG, (b) PCC in presence of 4 w/v% PEG-6000, (c) PCC in presence of 7 w/v% PEG-6000.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Concentration Assay

(A) SEM image of PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (B) 30 000× of SEM image (A), (C) particle size distribution of PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (D) SEM micro-image of PCC particles from with 0.03 M salt concentration and 1.5 w/v% PSS, (E) 30 000× magnification of SEM image (D), (F) particle size distribution of PCC from 0.03 M salt concentration and 1.5 w/v% PSS. (G) XRD fingerprints, (H) ATR spectra and (I) Raman spectra of (a) PCC in presence of 7 w/v% PEG-6000 and (b) PCC in presence of 1.5 w/v% PSS.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: (A) SEM image of PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (B) 30 000× of SEM image (A), (C) particle size distribution of PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (D) SEM micro-image of PCC particles from with 0.03 M salt concentration and 1.5 w/v% PSS, (E) 30 000× magnification of SEM image (D), (F) particle size distribution of PCC from 0.03 M salt concentration and 1.5 w/v% PSS. (G) XRD fingerprints, (H) ATR spectra and (I) Raman spectra of (a) PCC in presence of 7 w/v% PEG-6000 and (b) PCC in presence of 1.5 w/v% PSS.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Concentration Assay

(A) SEM image of PCC particles from 0.03 M salt concentration, in presence of 7 w/v% PEG-6000 and 0.01 M silver colloid, (B) 30 000× of SEM image (A), (C) SEM image of PCC from 0.03 M salt concentration, 1.5 w/v% PSS and 0.01 M silver colloid, (D) particle size distribution of PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (E) particle size distribution of silver nanoparticles deposited on PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (F) particle size distribution of PCC from 0.03 M salt concentration and 1.5 w/v% PSS. (G) XRD fingerprints and (H) ATR spectra of (a) PCC particles from of 0.03 M salt concentration, 7 w/v% PEG-6000 and 0.01 M silver colloid and (b) PCC particles from of 0.03 M salt concentration, 1.5 w/v% PSS and 0.01 M silver colloid.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: (A) SEM image of PCC particles from 0.03 M salt concentration, in presence of 7 w/v% PEG-6000 and 0.01 M silver colloid, (B) 30 000× of SEM image (A), (C) SEM image of PCC from 0.03 M salt concentration, 1.5 w/v% PSS and 0.01 M silver colloid, (D) particle size distribution of PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (E) particle size distribution of silver nanoparticles deposited on PCC from 0.03 M salt concentration and 7 w/v% PEG-6000, (F) particle size distribution of PCC from 0.03 M salt concentration and 1.5 w/v% PSS. (G) XRD fingerprints and (H) ATR spectra of (a) PCC particles from of 0.03 M salt concentration, 7 w/v% PEG-6000 and 0.01 M silver colloid and (b) PCC particles from of 0.03 M salt concentration, 1.5 w/v% PSS and 0.01 M silver colloid.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Concentration Assay

(A) SEM image of PCC particles from 0.03 M salt concentration, with 7 w/v% PEG-6000 and 0.01 M silver colloid, (B) Ca EDS image mapping, (C) silver EDS mapping image, (D) SEM image of PCC particles from 0.03 M salt concentration, with 1.5 w/v% PSS and 0.01 M silver colloid, (E) Ca EDS mapping image and (F) silver mapping image.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: (A) SEM image of PCC particles from 0.03 M salt concentration, with 7 w/v% PEG-6000 and 0.01 M silver colloid, (B) Ca EDS image mapping, (C) silver EDS mapping image, (D) SEM image of PCC particles from 0.03 M salt concentration, with 1.5 w/v% PSS and 0.01 M silver colloid, (E) Ca EDS mapping image and (F) silver mapping image.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Concentration Assay

(A) AFM micro-images of PCC particles in PSS, (B) PCC particles loaded with silver nanoparticles in PSS, (C) nitrogen adsorption–desorption isotherms of (a) untreated ground eggshell particles, (b) PCC particles in PSS, and (c) PCC particles loaded with silver nanoparticles in PSS.

Journal: RSC Advances

Article Title: Tuning polymorphs of precipitated calcium carbonate from discarded eggshells: effects of polyelectrolyte and salt concentration

doi: 10.1039/d2ra01673g

Figure Lengend Snippet: (A) AFM micro-images of PCC particles in PSS, (B) PCC particles loaded with silver nanoparticles in PSS, (C) nitrogen adsorption–desorption isotherms of (a) untreated ground eggshell particles, (b) PCC particles in PSS, and (c) PCC particles loaded with silver nanoparticles in PSS.

Article Snippet: Attenuated total reflection (ATR) spectra of PCC particles were recorded from Bruker Tensor 27 spectrophotometer at ambient temperature.

Techniques: Adsorption