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The M‐candles and characterizations of the SACs library. (a) Schematic of the metal‐paraffin “M‐candle” used for one‐step soot deposition of SA–M–CS coatings. <t>(b)</t> <t>HAADF‐STEM</t> images of SA–M–CS SACs showing atomically dispersed metal sites on graphitic carbon nanospheres: scale bar, 2 nm. (c) FT‐EXAFS spectra (gray) with corresponding fitting (red) of SA–M–CS SACs, confirming single‐atom coordination environments; insets depict the dominant coordination motifs.
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The M‐candles and characterizations of the SACs library. (a) Schematic of the metal‐paraffin “M‐candle” used for one‐step soot deposition of SA–M–CS coatings. <t>(b)</t> <t>HAADF‐STEM</t> images of SA–M–CS SACs showing atomically dispersed metal sites on graphitic carbon nanospheres: scale bar, 2 nm. (c) FT‐EXAFS spectra (gray) with corresponding fitting (red) of SA–M–CS SACs, confirming single‐atom coordination environments; insets depict the dominant coordination motifs.
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a Schematic illustration of the preparation of Au/TiO 2 @pSiO 2 -X catalysts. The black dashed box highlights the template agents used in material synthesis: C 12 TAB, dodecyltrimethylammonium bromide; C 16 TAB, cetyltrimethylammonium bromide. b HR-TEM image of Au/TiO 2 @pSiO 2 -1.7 catalysts. The white dashed line outlines the porous SiO 2 shell, and the white arrow points to the SiO 2 shell. c A High-angle annular dark-field scanning transmission electron microscopy <t>(HAADF-STEM)</t> image of Au/TiO 2 @pSiO 2 -1.7 catalysts. White arrows point to the highly dispersed Au NP and TiO 2 core, respectively. d EDS mapping images of Au/TiO 2 @pSiO 2 -1.7. Different colors correspond to different elements (red: Ti; green: Si; yellow: Au; cyan: O). e N 2 adsorption-desorption isotherms of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. f Pore size distribution of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. g UV-Vis DRS of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X.
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a Schematic illustration of the preparation of Au/TiO 2 @pSiO 2 -X catalysts. The black dashed box highlights the template agents used in material synthesis: C 12 TAB, dodecyltrimethylammonium bromide; C 16 TAB, cetyltrimethylammonium bromide. b HR-TEM image of Au/TiO 2 @pSiO 2 -1.7 catalysts. The white dashed line outlines the porous SiO 2 shell, and the white arrow points to the SiO 2 shell. c A High-angle annular dark-field scanning transmission electron microscopy <t>(HAADF-STEM)</t> image of Au/TiO 2 @pSiO 2 -1.7 catalysts. White arrows point to the highly dispersed Au NP and TiO 2 core, respectively. d EDS mapping images of Au/TiO 2 @pSiO 2 -1.7. Different colors correspond to different elements (red: Ti; green: Si; yellow: Au; cyan: O). e N 2 adsorption-desorption isotherms of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. f Pore size distribution of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. g UV-Vis DRS of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X.
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The M‐candles and characterizations of the SACs library. (a) Schematic of the metal‐paraffin “M‐candle” used for one‐step soot deposition of SA–M–CS coatings. (b) HAADF‐STEM images of SA–M–CS SACs showing atomically dispersed metal sites on graphitic carbon nanospheres: scale bar, 2 nm. (c) FT‐EXAFS spectra (gray) with corresponding fitting (red) of SA–M–CS SACs, confirming single‐atom coordination environments; insets depict the dominant coordination motifs.

Journal: Advanced Materials (Deerfield Beach, Fla.)

Article Title: Scalable and Customizable Single‐Atom Coatings for pH‐Universal H 2 O 2 Electrosynthesis

doi: 10.1002/adma.202521237

Figure Lengend Snippet: The M‐candles and characterizations of the SACs library. (a) Schematic of the metal‐paraffin “M‐candle” used for one‐step soot deposition of SA–M–CS coatings. (b) HAADF‐STEM images of SA–M–CS SACs showing atomically dispersed metal sites on graphitic carbon nanospheres: scale bar, 2 nm. (c) FT‐EXAFS spectra (gray) with corresponding fitting (red) of SA–M–CS SACs, confirming single‐atom coordination environments; insets depict the dominant coordination motifs.

Article Snippet: Atomic‐resolution HAADF‐STEM images and the corresponding EDS mappings were taken on a JEOL Grand ARM (JEM‐ARM300F) STEM with double correctors operated at 300 keV.

Techniques:

a Schematic illustration of the preparation of Au/TiO 2 @pSiO 2 -X catalysts. The black dashed box highlights the template agents used in material synthesis: C 12 TAB, dodecyltrimethylammonium bromide; C 16 TAB, cetyltrimethylammonium bromide. b HR-TEM image of Au/TiO 2 @pSiO 2 -1.7 catalysts. The white dashed line outlines the porous SiO 2 shell, and the white arrow points to the SiO 2 shell. c A High-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) image of Au/TiO 2 @pSiO 2 -1.7 catalysts. White arrows point to the highly dispersed Au NP and TiO 2 core, respectively. d EDS mapping images of Au/TiO 2 @pSiO 2 -1.7. Different colors correspond to different elements (red: Ti; green: Si; yellow: Au; cyan: O). e N 2 adsorption-desorption isotherms of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. f Pore size distribution of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. g UV-Vis DRS of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X.

Journal: Nature Communications

Article Title: Simultaneous promotion of photocatalytic CH 4 conversion and H 2 O 2 production via nanopore water confinement

doi: 10.1038/s41467-026-69719-z

Figure Lengend Snippet: a Schematic illustration of the preparation of Au/TiO 2 @pSiO 2 -X catalysts. The black dashed box highlights the template agents used in material synthesis: C 12 TAB, dodecyltrimethylammonium bromide; C 16 TAB, cetyltrimethylammonium bromide. b HR-TEM image of Au/TiO 2 @pSiO 2 -1.7 catalysts. The white dashed line outlines the porous SiO 2 shell, and the white arrow points to the SiO 2 shell. c A High-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) image of Au/TiO 2 @pSiO 2 -1.7 catalysts. White arrows point to the highly dispersed Au NP and TiO 2 core, respectively. d EDS mapping images of Au/TiO 2 @pSiO 2 -1.7. Different colors correspond to different elements (red: Ti; green: Si; yellow: Au; cyan: O). e N 2 adsorption-desorption isotherms of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. f Pore size distribution of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X. g UV-Vis DRS of Au/TiO 2 and Au/TiO 2 @pSiO 2 -X.

Article Snippet: High-resolution TEM (HRTEM) images, HAADF-STEM images, and corresponding EDS maps were collected using a JEOL JEM-F200 field-emission microscope operated at 200 kV.

Techniques: Transmission Assay, Electron Microscopy, Adsorption, Pore Size