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Overview of SPMESH-DART-MS/MS extraction and analysis approach including optimized sample preparation, SPMESH extraction, and DART-MS/MS parameters in this study.

Journal: Molecules

Article Title: Optimized Solid-Phase Mesh-Enhanced Sorption from Headspace (SPMESH) for Rapid Sub-ng/kg Measurements of 3-Isobutyl-2-methoxypyrazine (IBMP) in Grapes

doi: 10.3390/molecules27196195

Figure Lengend Snippet: Overview of SPMESH-DART-MS/MS extraction and analysis approach including optimized sample preparation, SPMESH extraction, and DART-MS/MS parameters in this study.

Article Snippet: For SPMESH-DART-HRMS/MS analysis, web-based DART software (version 6.0.5, IonSense Inc., Saugus, MA, USA) was used to manually move the SPMESH sheet on the DART positioning stage unidirectionally through the DART reaction zone at 0.5 mm/sec at a desorption temperature of 350 °C in front of the MS inlet.

Techniques: Tandem Mass Spectroscopy, Sample Prep

Correlation between IBMP measured by SPMESH-DART-Orbitrap MS/MS and HS-SPME-GC-MS. Undetectable values were set to the square root of the LOD (SPME-GC-MS = 1.2 ng/kg, SPMESH-DART-MS = 0.71 ng/kg).

Journal: Molecules

Article Title: Optimized Solid-Phase Mesh-Enhanced Sorption from Headspace (SPMESH) for Rapid Sub-ng/kg Measurements of 3-Isobutyl-2-methoxypyrazine (IBMP) in Grapes

doi: 10.3390/molecules27196195

Figure Lengend Snippet: Correlation between IBMP measured by SPMESH-DART-Orbitrap MS/MS and HS-SPME-GC-MS. Undetectable values were set to the square root of the LOD (SPME-GC-MS = 1.2 ng/kg, SPMESH-DART-MS = 0.71 ng/kg).

Article Snippet: For SPMESH-DART-HRMS/MS analysis, web-based DART software (version 6.0.5, IonSense Inc., Saugus, MA, USA) was used to manually move the SPMESH sheet on the DART positioning stage unidirectionally through the DART reaction zone at 0.5 mm/sec at a desorption temperature of 350 °C in front of the MS inlet.

Techniques: Tandem Mass Spectroscopy, Gas Chromatography-Mass Spectrometry