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Structures of dihydroxyphenazine sulfonate (DHPS), 5-hydroxy-benzo[ a ]phenazine-sulfonic acid (BHPS), iron-2,2-bis(hydroxymethyl)-2,2′,2′-nitrilotriethanol (Fe Bis-Tris), iron-3-[bis(2-hydroxyethyl)amino]-2-hydroxypropanesulfonic acid (Fe DIPSO), the four redox mediators evaluated in this work. Each structure is labelled.

Journal: Faraday Discussions

Article Title: Electrolysis without electrodes: thermodynamic and kinetic insights into decoupled alkaline water electrolysis

doi: 10.1039/d6fd00117c

Figure Lengend Snippet: Structures of dihydroxyphenazine sulfonate (DHPS), 5-hydroxy-benzo[ a ]phenazine-sulfonic acid (BHPS), iron-2,2-bis(hydroxymethyl)-2,2′,2′-nitrilotriethanol (Fe Bis-Tris), iron-3-[bis(2-hydroxyethyl)amino]-2-hydroxypropanesulfonic acid (Fe DIPSO), the four redox mediators evaluated in this work. Each structure is labelled.

Article Snippet: Iron-2,2-bis(hydroxymethyl)-2,2′,2′-nitrilotriethanol (98%, Bis-Tris), 3-[bis(2-hydroxyethyl)amino]-2-hydroxypropanesulfonic acid (99%, DIPSO), potassium ferrocyanide (99%), nickel powder APS 2.2–3 micron and nickel powder APS 3–7 micron (APS, atmospheric plasma spraying, 99.9%), and acetone were purchased from Thermo Fisher Scientific (Alfa Aesar, Acros Organics).

Techniques:

(A) Overlay of cyclic voltammograms for a selection of alkaline soluble redox mediators in 4 M NaOH. Working electrode was glassy carbon, reference electrode was Hg/HgO and the counter was a platinum wire. Scan rate is 20 mV s −1 and solutions were deoxygenated. (B) Overlay of the theoretical Nernst profile for the changing state of charge for each redox mediator. The redox mediators abbreviated in the figure legends are dihydroxyphenazine sulfonate (DHPS), 5-hydroxy-benzo[ a ]phenazine-sulfonic acid (BHPS), iron-2,2-bis(hydroxymethyl)-2,2′,2′-nitrilotriethanol (Fe Bis-Tris), iron-3-[bis(2-hydroxyethyl)amino]-2-hydroxypropanesulfonic acid (Fe DIPSO).

Journal: Faraday Discussions

Article Title: Electrolysis without electrodes: thermodynamic and kinetic insights into decoupled alkaline water electrolysis

doi: 10.1039/d6fd00117c

Figure Lengend Snippet: (A) Overlay of cyclic voltammograms for a selection of alkaline soluble redox mediators in 4 M NaOH. Working electrode was glassy carbon, reference electrode was Hg/HgO and the counter was a platinum wire. Scan rate is 20 mV s −1 and solutions were deoxygenated. (B) Overlay of the theoretical Nernst profile for the changing state of charge for each redox mediator. The redox mediators abbreviated in the figure legends are dihydroxyphenazine sulfonate (DHPS), 5-hydroxy-benzo[ a ]phenazine-sulfonic acid (BHPS), iron-2,2-bis(hydroxymethyl)-2,2′,2′-nitrilotriethanol (Fe Bis-Tris), iron-3-[bis(2-hydroxyethyl)amino]-2-hydroxypropanesulfonic acid (Fe DIPSO).

Article Snippet: Iron-2,2-bis(hydroxymethyl)-2,2′,2′-nitrilotriethanol (98%, Bis-Tris), 3-[bis(2-hydroxyethyl)amino]-2-hydroxypropanesulfonic acid (99%, DIPSO), potassium ferrocyanide (99%), nickel powder APS 2.2–3 micron and nickel powder APS 3–7 micron (APS, atmospheric plasma spraying, 99.9%), and acetone were purchased from Thermo Fisher Scientific (Alfa Aesar, Acros Organics).

Techniques: Selection, Platinum