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FESEM of the investigated powders; a , b Al 2 O 3 short fibers, c Mo, d Zr, e Ti, f – h mechanically alloyed powdered material after ball milling, i , j EDAX elemental composition analysis produced powders of Al 2 O 3 short fibers/Ti-12Mo-6Zr and Ti-12Mo-6Zr composites after wet milling in ethanol for 24 h

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: FESEM of the investigated powders; a , b Al 2 O 3 short fibers, c Mo, d Zr, e Ti, f – h mechanically alloyed powdered material after ball milling, i , j EDAX elemental composition analysis produced powders of Al 2 O 3 short fibers/Ti-12Mo-6Zr and Ti-12Mo-6Zr composites after wet milling in ethanol for 24 h

Article Snippet: Fig. 8 a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min Fig. 9 a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Techniques: Produced, Wet-Milling

FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min

Article Snippet: Fig. 8 a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min Fig. 9 a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Techniques:

a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min

Article Snippet: Fig. 8 a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min Fig. 9 a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Techniques:

a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Article Snippet: Fig. 8 a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min Fig. 9 a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Techniques:

FESEM of the investigated powders; a , b Al 2 O 3 short fibers, c Mo, d Zr, e Ti, f – h mechanically alloyed powdered material after ball milling, i , j EDAX elemental composition analysis produced powders of Al 2 O 3 short fibers/Ti-12Mo-6Zr and Ti-12Mo-6Zr composites after wet milling in ethanol for 24 h

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: FESEM of the investigated powders; a , b Al 2 O 3 short fibers, c Mo, d Zr, e Ti, f – h mechanically alloyed powdered material after ball milling, i , j EDAX elemental composition analysis produced powders of Al 2 O 3 short fibers/Ti-12Mo-6Zr and Ti-12Mo-6Zr composites after wet milling in ethanol for 24 h

Article Snippet: Fig. 5 FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min Figure shows the EDAX analysis of the Ti particles during the first stage of the sintering.

Techniques: Produced, Wet-Milling

FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min

Article Snippet: Fig. 5 FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min Figure shows the EDAX analysis of the Ti particles during the first stage of the sintering.

Techniques:

a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: a – f FESEM microstructure images with low and high magnifications, g , h EDAX elemental compositional analysis of the Widmannstatten-like microstructure of the prepared Ti-12Mo-6Zr biomaterial by SPS at 1000 o C and 50 MPa for 5 min

Article Snippet: Fig. 5 FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min Figure shows the EDAX analysis of the Ti particles during the first stage of the sintering.

Techniques:

a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Journal: Journal of Materials Science. Materials in Medicine

Article Title: Novel synthesis of Al 2 O 3 short fibers/Ti-12Mo-6Zr composites for cranial reconstruction applications: spark plasma sintering, microstructure and nanomechanical properties

doi: 10.1007/s10856-025-06919-x

Figure Lengend Snippet: a , b FESEM microstructure images of 1 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr and 2.5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites, ( c – e ) the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites with different magnifications, f the Al6MoTi dendrite phase, g high magnification of the interface between the Al 2 O 3 short fibers and the metal matrix and h the EDAX elemental analysis of the 5 wt.% Al 2 O 3 short fibers/Ti-12Mo-6Zr composites prepared by SPS at 1000 o C and 50 MPa for 5 min

Article Snippet: Fig. 5 FESEM images with secondary electron ( a , c , e , f ), back scattering modes ( b , d ) and EDAX elemental compositional analysis ( g , h ) of the sintering stages of the prepared Ti-12Mo-6Zr composites by SPS at 1000 o C and 50 MPa for 5 min Figure shows the EDAX analysis of the Ti particles during the first stage of the sintering.

Techniques: